The Analysis of Water for Perfluorinated Compounds using Automated Solid Phase Extraction

Characterization of Polyfluoroalkyl Substances in the Environment
Oral Presentation

Prepared by , M. Ebitson, A. Cannon, W. Jones

Contact Information: [email protected]; 603-386-3654


Perfluorinated compounds (PFCs) are of increasing concern as they are detected in environmental and human samples. Originally thought to be inert compounds, they are long-lived and may cause tumors and endocrine effects. They bioaccumulate so continued exposure may be especially hazardous. The measurement of PFCs was included in the Unregulated Contaminant Monitoring Program 3 (UCMR-3) and occurrence evaluated in drinking water across the US. US EPA Method 537, which passes 250 mL of water through a cartridge and subsequent analysis with LC/MS/MS, was developed to support this effort. As reports of PFC contamination continue to draw headlines, the need for a simple and automated analysis becomes more critical.

This work evaluates the development of automated methodology for EPA 537. Background levels and the need to develop a system that will minimize contamination will be discussed. A range of water samples will be analyzed and challenges and results presented.