Draft Practice for Development and Optimization of D19 Chemical Analysis Methods Intended for EPA Compliance Reporting

ASTM Committee D-19s Effort to Provide Useful Test Methods to the Environmental Laboratory Community
Oral Presentation

Prepared by

Contact Information: jerry.parr@nelac-institute.org; 817-598-1624


ABSTRACT

ASTM D-2777 provides the standard practice for conducting an interlaboratory study to determine the precision and bias of a test method. However, no such practice exists for the initial development of a method to be used for compliance purposes. Method development cannot be prescriptive. This is a guide of suggested practices. Because methods vary widely in their chemistry and procedures, no definitive guidance can be provided on how to develop a rugged method. In general, though, the goal is a written document that demonstrates acceptable method performance is attained using all procedural options specified in the method.